Equipment

 
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Two high-resolution pulse NMR spectrometers are avialable in our laboratory:

Bruker 600 AvanceIII

Triple-resonance digital NMR spectrometer with the following parameters:

  • actively shielded superconducting magnet UltraShield™ 14.1 T
  • digital console
  • orthogonal BOSS II shimming system with 34 gradients
  • two probeheads:
    • 5 mm triple-resonance cryoprobe TCI (1H observe, 13C and 15N manipulation, deuterium decoupling possible), actively shielded z-gradient
    • 5 mm TXI – triple-resonance probehead for inverse experiments (1H observe, 13C and 15N manipulation), actively shielded z-gradient

Bruker Avance DRX 500

in the configuration as a three-channel high performance Fourier NMR spectrometer equipped with
  • three axis (x, y, z) gradient unit capable of delivering a gradient of up to 50 G/cm
  • fully digital console (digital lock controling unit, digital quadrature detection)
  • Bruker orthogonal shim system BOSS II (28 shim gradients)
  • three special probeheads
    • 1H, 13C, 19F, 31P QNP 5 mm probehead with actively shielded z-gradient coil
    • triple resonance inverse 5 mm probehead (1H observe, BB/13C decoupling) with xyz-gradients
    • 10 mm broadband probehead in the standard range (31P - 109Ag), 1H decoupling

Bruker AMX-3 400 is no longer in use!!


The spectrometer is operated using SGI Indy workstations.