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NMR spectroscopy in Natural Compounds

Lecture Excercise/laboratory
2020, Summer Semester
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Credits 3
Hours per week 2 / 1 / 0
Examination MC
Study Language Czech
Level []
Guarantor Ing. Hana Dvořáková, CSc.
prof. Ing. Richard Hrabal, CSc.
Ing. Jan Prchal, Ph.D.
Supplemental electronic materials available at UCT Prague's e-learning

Summary

The purpose of the course is to teach students the fundaments of Nuclear magnetic resonance spectroscopy. It is designed for NMR users to be able to choose a proper NMR experiment, to set it up on an NMR spectrometer, process the results and interpret the spectra. The course is divided into three sections, the first one is about physical background of NMR, the second one is devoted to principles of interpretation of NMR spectra and the last one should help students to orient themselves in numerous applications of NMR spectroscopy. Students must work out their own projects to successfully pass the course.

Syllabus

1. Basic concepts, principle of pulse experiments
2. Two- and multidimensional NMR
3. Nuclear relaxation, chemical exchange, NOE effect
4. Construction and basis of operation of NMR spectrometers
5. Interpretation of NMR spectra, calculations, databases
6. Conformational analysis I
7. Conformational analysis II
8. Chemical exchange
9. Multi-nuclear NMR and its application for solving particular problems
10. Examination project assignment
11. NMR of biologically active systems
12. Study of non-bonding interactions
13. Quantitative NMR, magnetic resonance imaging
14. Solid-state NMR

Literature

R: H. Friebolin: Basic One- and Two-Dimensional NMR Spectroscopy, Wiley-VCH, 4. edition, 2005
A: H. Günther: NMR Spectrsocopy John Wileay and Sons, 2.edition, 2001

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