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Data for 2017/2018

Methods of Structural and Surface Analysis

Credits 3
Hours per week 2 / 0 / 0
Examination Ex
Study Language Czech
Level Master subject
Guarantor prof. Dr. RNDr. Pavel Matějka

Summary

This subject comprises the basic terms, related to the molecular structure analysis and surface analysis. It brings a survey of individual techniques and offered information. Techniques of the surface analysis and imaging, including the scanning probe (near-field) microanalysis, are the second key part of this survey. In some cases it is an extension of knowledge gained in the basic courses of Analytical chemistry I and II.

Syllabus

1. Fundamental terms
2. Structure and geometry of molecules
3. Symmetry, point groups
4. Linear and circular polarized electromagnetic radiation, chirooptical methods
5. Infrared and Raman spectroscopy
6. Microwave spectroscopy
7. NMR spectrometry
8. Mass spectrometry
9. Crystal structure
10. X-ray and electron diffraction
11. Surface analysis methods based on electron detection
12. Surface analysis methods based on ion detection
13. Surface analysis methods based on photon detection
14. Scanning microscopy methods

Literature

R: R.L. McCreery: Raman Spectroscopy for Chemical Analysis, Wiley 2000 (available online at VSCHT)
Modern Instrumental Analysis, ed. S. Ahuja, N. Jespersen, Comprehensive Analytical Chemistry Vol. 47 (2006), p. 1-864 (available online at VSCHT)
A: Non-Destrictive Microanalysis of Cultural Heritage materials, ed. S. Ahuja, N. Jespersen, Comprehensive Analytical Chemistry Vol. 42 (2004), p. 1-800 (available online at VSCHT)
A: L. A. Casper, C. J. Powell: Industrial Applications of Surface Analysis, vol. 199, ACS 1982 (available online at VSCHT)

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Datová schránka: sp4j9ch

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